Jan 25, 2019 · In brief, ZrCl 4 (0.795 g, 3.411 mmol) and terephthalic acid (0.566 g, 3.411 mmol) were dissolved in 250 mL of DMF by sonication at room temperature. 15 mL of acetic acid were added to the obtained mixture that was put in a 500 mL autoclavable reagent bottle and placed in a pre-heated oven at 120 °C for 21 h. The obtained white precipitate was
Screw Neck Purification Reagent Bottle Petroleum Industry Fisher
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