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The laboratory bottles designed for top space analysis is what we call headspace vials. The essence of this experiment is that the volatile sample is heated and volatilized to form gas in the space at the top of the sample bottle and then diffuse, and finally the top gas in the gas chromatographic bottle above the volatile sample enters the gas phase detection.

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Page 8First Steps Mounting and Screw the instrument (GL 45 thread) onto the reagent bottle and then align aligning the instru- ment on a bottle the discharge tube with the bottle label by turning the valve block (Fig. 3). To prevent tipping over use a bottle stand for small bottles (page 46). Page 9: Priming.